NMR Spectroscopy

 Overview of the NMR sprectrometer in our group. Responsible for NMR in our group is Dr. Harald Scherer (liquid) Dr. Anke Schaub (MAS).


Bruker Avance II WB 400 MHz

magnet: wide bore (Bruker UltraShieldPlus, 9.4 Tesla)
sample head:

ATM BBFO Breitband 5 mm, 5 mm TBI, 4 mm MAS

operation: manual and with auto sampler
gradient: Z-gradienten unit and gradient shim  
temperature unit:

down to -70 °C with liquid nitrogen and from +150 °C to -140 °C (for MAS)

sample changer: BACS 60
nuclei:

1H, 19F, 31P - 109Ag (for high resolution)

1H, 19F, 31P - 33S (for MAS)


Bruker Avance III HD 300 MHz

magnet:

normal bore (Bruker ultrashield, 7.04 T)                                                            

 sample head:

5 mm ATM BBFO

operation: manual and with auto sampler
gradient: Z-gradienten unit and gradient shim  
temperature unit:

BCU I or liquid nitrogen

sample changer:

SampleXpress Lite

nuclei:

1H, 19F, 31P - 109Ag (for high resolution)

 

1H, 19F, 31P - 33S (for MAS)


Bruker DPX 200 MHz

magnet: normal bore (Bruker, 4.7 Tesla)                                                                             
sample head: QNP 5 mm (1H, 19F, 31P, 13C)
operation: manual and with auto sampler
gradient: Z-gradienten unit
temperature unit:

down to -70 °C with liquid nitrogen

nuclei:

1H, 19F, 31P, 13C

sample changer:

Bruker SIXPACK